教學大綱表 (111學年度 第1學期)
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課程名稱
Course Title
(中文) 有機分析化學
(英文) Organic Analysis Chemistry Organic Analysis
開課單位
Departments
化學工程與生物科技學系
課程代碼
Course No.
C3200
授課教師
Instructor
黃俊誠
學分數
Credit
3.0 必/選修
core required/optional
選修 開課年級
Level
大三
先修科目或先備能力(Course Pre-requisites):有機化學和儀器分析
課程概述與目標(Course Overview and Goals): 課程概述與目標: 介紹IR、UV、mass及NMR光譜分析法之原理,並將之應用於有機化合物的化學結構之鑑定
教科書(Textbook) Spectroscopy, 4th Ed., Lampman, Pavia, Kriz, Vyvyan, Brooks/Cole, 2010
參考教材(Reference) 1. Introduction to Spectroscopy, 3rd Ed., Pavia, Lampman, Kriz, Brooks/Cole, 2001.
2. Spectrometric Identification of Organic Compounds, 7th Ed., Robert M. Silverstein, Francis X. Webster, David J. Kiemle
課程大綱 Syllabus 學生學習目標
Learning Objectives
單元學習活動
Learning Activities
學習成效評量
Evaluation
備註
Notes

No.
單元主題
Unit topic
內容綱要
Content summary
1 Molecular Formula and What can be Learned from them 1. Elemental analysis and calculation
2. Determination of molecular mass
3. Molecular formula
4. Index of hydrogen deficiency
5. The rule of thirteen
有機分析化學基礎概念學習  
2 Molecular Formula and What can be Learned from them 1. Elemental analysis and calculation
2. Determination of molecular mass
3. Molecular formula
4. Index of hydrogen deficiency
5. The rule of thirteen
有機分析化學基礎概念學習  
3 Infrared Spectroscopy 1. The infrared absorption process
2. The modes of stretching and bending
3. Bond properties and absorption trends
4. The infrared spectrometer
5. How to approach the analysis of a spectrum
學習如何以紅外線光譜分析化合物官能基  
4 Infrared Spectroscopy 1. The infrared absorption process
2. The modes of stretching and bending
3. Bond properties and absorption trends
4. The infrared spectrometer
5. How to approach the analysis of a spectrum
學習如何以紅外線光譜分析化合物官能基  
5 Infrared Spectroscopy 1. The infrared absorption process
2. The modes of stretching and bending
3. Bond properties and absorption trends
4. The infrared spectrometer
5. How to approach the analysis of a spectrum
學習如何以紅外線光譜分析化合物官能基  
6 Infrared Spectroscopy 1. The infrared absorption process
2. The modes of stretching and bending
3. Bond properties and absorption trends
4. The infrared spectrometer
5. How to approach the analysis of a spectrum
學習如何以紅外線光譜分析化合物官能基  
7 Infrared Spectroscopy 1. The infrared absorption process
2. The modes of stretching and bending
3. Bond properties and absorption trends
4. The infrared spectrometer
5. How to approach the analysis of a spectrum
學習如何以紅外線光譜分析化合物官能基  
8 Infrared Spectroscopy 1. The infrared absorption process
2. The modes of stretching and bending
3. Bond properties and absorption trends
4. The infrared spectrometer
5. How to approach the analysis of a spectrum
學習如何以紅外線光譜分析化合物官能基  
9 期中考 期中考 期中考  
10 1H NMR Spectroscopy 1. Basic concepts
2. The mechanism of resonance
3. The chemical shift and shielding
4. Local diamagnetic shielding
5. Magnetic anisotropy
6. Spin-spin splitting
7. Survey of typical proton NMR absorption by type of compound
學習如何以氫核磁共振光譜分析化合物結構  
11 1H NMR Spectroscopy 1. Basic concepts
2. The mechanism of resonance
3. The chemical shift and shielding
4. Local diamagnetic shielding
5. Magnetic anisotropy
6. Spin-spin splitting
7. Survey of typical proton NMR absorption by type of compound
學習如何以氫核磁共振光譜分析化合物結構  
12 1H NMR Spectroscopy 1. Basic concepts
2. The mechanism of resonance
3. The chemical shift and shielding
4. Local diamagnetic shielding
5. Magnetic anisotropy
6. Spin-spin splitting
7. Survey of typical proton NMR absorption by type of compound
學習如何以氫核磁共振光譜分析化合物結構  
13 1H NMR Spectroscopy 1. Basic concepts
2. The mechanism of resonance
3. The chemical shift and shielding
4. Local diamagnetic shielding
5. Magnetic anisotropy
6. Spin-spin splitting
7. Survey of typical proton NMR absorption by type of compound
學習如何以氫核磁共振光譜分析化合物結構  
14 Carbon-13 NMR Spectra 1. Carbon-13 NMR shifts
2. Proton-decoupled carbon-13 spectra
3. Nuclear overhauser enhancement (NOE)
4. A quick dip into DEPT
5. Some sample spectra
學習如何以碳-13核磁共振光譜分析化合物結構  
15 Mass Spectrometry 1. The mass spectrum
2. Determination of molecular weight
3. Determination of molecular formula
4. Some fragmentation patterns
學習如何以質譜分析化合物結構  
16 Compound analysis total analysis for experimental data 學習如何分析與判斷未知物的結構  
17 Compound analysis total analysis for experimental data 學習如何分析與判斷未知物的結構  
18 期末考 期末考 期末考  


教學要點概述:
1.自編教材 Handout by Instructor:
□ 1-1.簡報 Slids
□ 1-2.影音教材 Videos
□ 1-3.教具 Teaching Aids
□ 1-4.教科書 Textbook
□ 1-5.其他 Other
□ 2.自編評量工具/量表 Educational Assessment
□ 3.教科書作者提供 Textbook

成績考核 Performance Evaluation: 其他評量:10%   問答:10%   報告:30%   作業:50%  

教學資源(Teaching Resources):
□ 教材電子檔(Soft Copy of the Handout or the Textbook)
□ 課程網站(Website)
教學相關配合事項:須修過普通化學、有機化學(一)(二)和儀器分析且皆通過的同學才能修課
扣考規定:http://eboard.ttu.edu.tw/ttuwebpost/showcontent-news.php?id=504