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課程名稱 (中文) 有機分析化學
(英文) Organic Analysis Chemistry Organic Analysis
開課單位 化學工程學系
課程代碼 C3200
授課教師 黃俊誠
學分數 3.0 必/選修 選修 開課年級 大三
先修科目或先備能力:有機化學和儀器分析
課程概述與目標: 課程概述與目標: 介紹IR、UV、mass及NMR光譜分析法之原理,並將之應用於有機化合物的化學結構之鑑定
教科書 Spectroscopy, 4th Ed., Lampman, Pavia, Kriz, Vyvyan, Brooks/Cole, 2010
參考教材 1. Introduction to Spectroscopy, 3rd Ed., Pavia, Lampman, Kriz, Brooks/Cole, 2001.
2. Spectrometric Identification of Organic Compounds, 7th Ed., Robert M. Silverstein, Francis X. Webster, David J. Kiemle
課程大綱 學生學習目標 單元學習活動 學習成效評量 備註
單元主題 內容綱要
1 Molecular Formula and What can be Learned from them 1. Elemental analysis and calculation
2. Determination of molecular mass
3. Molecular formula
4. Index of hydrogen deficiency
5. The rule of thirteen
有機分析化學基礎概念學習
  • 作業
  •  
    2 Molecular Formula and What can be Learned from them 1. Elemental analysis and calculation
    2. Determination of molecular mass
    3. Molecular formula
    4. Index of hydrogen deficiency
    5. The rule of thirteen
    有機分析化學基礎概念學習
  • 作業
  •  
    3 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業
  •  
    4 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業
  •  
    5 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業
  •  
    6 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業
  •  
    7 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業
  •  
    8 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 平時考
  • 作業
  •  
    9 期中考 期中考 期中考  
    10 1H NMR Spectroscopy 1. Basic concepts
    2. The mechanism of resonance
    3. The chemical shift and shielding
    4. Local diamagnetic shielding
    5. Magnetic anisotropy
    6. Spin-spin splitting
    7. Survey of typical proton NMR absorption by type of compound
    學習如何以氫核磁共振光譜分析化合物結構
  • 作業
  •  
    11 1H NMR Spectroscopy 1. Basic concepts
    2. The mechanism of resonance
    3. The chemical shift and shielding
    4. Local diamagnetic shielding
    5. Magnetic anisotropy
    6. Spin-spin splitting
    7. Survey of typical proton NMR absorption by type of compound
    學習如何以氫核磁共振光譜分析化合物結構
  • 作業
  •  
    12 1H NMR Spectroscopy 1. Basic concepts
    2. The mechanism of resonance
    3. The chemical shift and shielding
    4. Local diamagnetic shielding
    5. Magnetic anisotropy
    6. Spin-spin splitting
    7. Survey of typical proton NMR absorption by type of compound
    學習如何以氫核磁共振光譜分析化合物結構
  • 作業
  •  
    13 1H NMR Spectroscopy 1. Basic concepts
    2. The mechanism of resonance
    3. The chemical shift and shielding
    4. Local diamagnetic shielding
    5. Magnetic anisotropy
    6. Spin-spin splitting
    7. Survey of typical proton NMR absorption by type of compound
    學習如何以氫核磁共振光譜分析化合物結構
  • 作業
  •  
    14 Carbon-13 NMR Spectra 1. Carbon-13 NMR shifts
    2. Proton-decoupled carbon-13 spectra
    3. Nuclear overhauser enhancement (NOE)
    4. A quick dip into DEPT
    5. Some sample spectra
    學習如何以碳-13核磁共振光譜分析化合物結構
  • 作業
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    15 Mass Spectrometry 1. The mass spectrum
    2. Determination of molecular weight
    3. Determination of molecular formula
    4. Some fragmentation patterns
    學習如何以質譜分析化合物結構  
    16 Compound anylsis total anylsis for experimetal data 學習如何分析與判斷未知物的結構
  • 討論
  • 講授
  • 個別或小組指導
  • 平時考
  • 作業
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    17 Compound anylsis total anylsis for experimetal data 學習如何分析與判斷未知物的結構
  • 討論
  • 個別或小組指導
  • 講授
  • 平時考
  • 作業
  •  
    18 期末考 期末考 期末考
  • 期末考
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    教學要點概述:
    教材編選: □ 自編教材 □ 教科書作者提供
    評量方法: 期末考:25%   期中考:25%   平時考:30%   作業:20%  
    教學資源: □ 教材電子檔 □ 課程網站
    教學相關配合事項:須修過有機化學(一)(二)和儀器分析且皆通過的同學才能修課
    扣考規定:http://eboard.ttu.edu.tw/ttuwebpost/showcontent-news.php?id=504