課程名稱 |
(中文) 有機分析化學 (英文) Organic Analysis Chemistry Organic Analysis |
開課單位 | 化學工程與生物科技學系 | ||
課程代碼 | C3200 | ||||
授課教師 | 黃俊誠 | ||||
學分數 | 3.0 | 必/選修 | 選修 | 開課年級 | 大三 |
先修科目或先備能力:有機化學和儀器分析 | |||||
課程概述與目標: 課程概述與目標: 介紹IR、UV、mass及NMR光譜分析法之原理,並將之應用於有機化合物的化學結構之鑑定 | |||||
教科書 | Spectroscopy, 4th Ed., Lampman, Pavia, Kriz, Vyvyan, Brooks/Cole, 2010 | ||||
參考教材 | 1. Introduction to Spectroscopy, 3rd Ed., Pavia, Lampman, Kriz, Brooks/Cole, 2001. 2. Spectrometric Identification of Organic Compounds, 7th Ed., Robert M. Silverstein, Francis X. Webster, David J. Kiemle |
課程大綱 | 學生學習目標 | 單元學習活動 | 學習成效評量 | 備註 | ||
週 | 單元主題 | 內容綱要 | ||||
1 | Molecular Formula and What can be Learned from them | 1. Elemental analysis and calculation 2. Determination of molecular mass 3. Molecular formula 4. Index of hydrogen deficiency 5. The rule of thirteen |
有機分析化學基礎概念學習 |
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2 | Molecular Formula and What can be Learned from them | 1. Elemental analysis and calculation 2. Determination of molecular mass 3. Molecular formula 4. Index of hydrogen deficiency 5. The rule of thirteen |
有機分析化學基礎概念學習 |
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3 | Infrared Spectroscopy | 1. The infrared absorption process 2. The modes of stretching and bending 3. Bond properties and absorption trends 4. The infrared spectrometer 5. How to approach the analysis of a spectrum |
學習如何以紅外線光譜分析化合物官能基 |
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4 | Infrared Spectroscopy | 1. The infrared absorption process 2. The modes of stretching and bending 3. Bond properties and absorption trends 4. The infrared spectrometer 5. How to approach the analysis of a spectrum |
學習如何以紅外線光譜分析化合物官能基 |
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5 | Infrared Spectroscopy | 1. The infrared absorption process 2. The modes of stretching and bending 3. Bond properties and absorption trends 4. The infrared spectrometer 5. How to approach the analysis of a spectrum |
學習如何以紅外線光譜分析化合物官能基 |
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6 | Infrared Spectroscopy | 1. The infrared absorption process 2. The modes of stretching and bending 3. Bond properties and absorption trends 4. The infrared spectrometer 5. How to approach the analysis of a spectrum |
學習如何以紅外線光譜分析化合物官能基 |
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7 | Infrared Spectroscopy | 1. The infrared absorption process 2. The modes of stretching and bending 3. Bond properties and absorption trends 4. The infrared spectrometer 5. How to approach the analysis of a spectrum |
學習如何以紅外線光譜分析化合物官能基 |
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8 | Infrared Spectroscopy | 1. The infrared absorption process 2. The modes of stretching and bending 3. Bond properties and absorption trends 4. The infrared spectrometer 5. How to approach the analysis of a spectrum |
學習如何以紅外線光譜分析化合物官能基 |
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9 | 期中考 | 期中考 | 期中考 | |||
10 | 1H NMR Spectroscopy | 1. Basic concepts 2. The mechanism of resonance 3. The chemical shift and shielding 4. Local diamagnetic shielding 5. Magnetic anisotropy 6. Spin-spin splitting 7. Survey of typical proton NMR absorption by type of compound |
學習如何以氫核磁共振光譜分析化合物結構 |
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11 | 1H NMR Spectroscopy | 1. Basic concepts 2. The mechanism of resonance 3. The chemical shift and shielding 4. Local diamagnetic shielding 5. Magnetic anisotropy 6. Spin-spin splitting 7. Survey of typical proton NMR absorption by type of compound |
學習如何以氫核磁共振光譜分析化合物結構 |
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12 | 1H NMR Spectroscopy | 1. Basic concepts 2. The mechanism of resonance 3. The chemical shift and shielding 4. Local diamagnetic shielding 5. Magnetic anisotropy 6. Spin-spin splitting 7. Survey of typical proton NMR absorption by type of compound |
學習如何以氫核磁共振光譜分析化合物結構 |
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13 | 1H NMR Spectroscopy | 1. Basic concepts 2. The mechanism of resonance 3. The chemical shift and shielding 4. Local diamagnetic shielding 5. Magnetic anisotropy 6. Spin-spin splitting 7. Survey of typical proton NMR absorption by type of compound |
學習如何以氫核磁共振光譜分析化合物結構 |
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14 | Carbon-13 NMR Spectra | 1. Carbon-13 NMR shifts 2. Proton-decoupled carbon-13 spectra 3. Nuclear overhauser enhancement (NOE) 4. A quick dip into DEPT 5. Some sample spectra |
學習如何以碳-13核磁共振光譜分析化合物結構 |
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15 | Mass Spectrometry | 1. The mass spectrum 2. Determination of molecular weight 3. Determination of molecular formula 4. Some fragmentation patterns |
學習如何以質譜分析化合物結構 | |||
16 | Compound analysis | total analysis for experimental data | 學習如何分析與判斷未知物的結構 |
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17 | Compound analysis | total analysis for experimental data | 學習如何分析與判斷未知物的結構 |
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18 | 期末考 | 期末考 | 期末考 |
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教學要點概述: |