教學大綱表 Syllabus
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課程名稱
Course Title
(中文) 有機分析化學
(英文) Organic Analysis Chemistry Organic Analysis
開課單位
Departments
化學工程與生物科技學系
課程代碼
Course No.
C3200
授課教師
Instructor
黃俊誠
學分數
Credit
3.0 必/選修
core required/optional
選修 開課年級
Level
大三
先修科目或先備能力Course Pre-requisites:有機化學和儀器分析
課程概述與目標 Course Overview and Goals: 課程概述與目標: 介紹IR、UV、mass及NMR光譜分析法之原理,並將之應用於有機化合物的化學結構之鑑定
教科書
Textbook
Spectroscopy, 4th Ed., Lampman, Pavia, Kriz, Vyvyan, Brooks/Cole, 2010
參考教材
Reference
1. Introduction to Spectroscopy, 3rd Ed., Pavia, Lampman, Kriz, Brooks/Cole, 2001.
2. Spectrometric Identification of Organic Compounds, 7th Ed., Robert M. Silverstein, Francis X. Webster, David J. Kiemle
課程大綱
Syllabus
學生學習目標
Learning Objectives
單元學習活動
Learning Activities
學習成效評量
Evaluation
備註
Notes

Week
單元主題
Unit topic
內容綱要
Content summary
1 Molecular Formula and What can be Learned from them 1. Elemental analysis and calculation
2. Determination of molecular mass
3. Molecular formula
4. Index of hydrogen deficiency
5. The rule of thirteen
有機分析化學基礎概念學習
  • 作業 Assignment
  •  
    2 Molecular Formula and What can be Learned from them 1. Elemental analysis and calculation
    2. Determination of molecular mass
    3. Molecular formula
    4. Index of hydrogen deficiency
    5. The rule of thirteen
    有機分析化學基礎概念學習
  • 作業 Assignment
  •  
    3 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業 Assignment
  •  
    4 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業 Assignment
  •  
    5 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業 Assignment
  •  
    6 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業 Assignment
  •  
    7 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 作業 Assignment
  •  
    8 Infrared Spectroscopy 1. The infrared absorption process
    2. The modes of stretching and bending
    3. Bond properties and absorption trends
    4. The infrared spectrometer
    5. How to approach the analysis of a spectrum
    學習如何以紅外線光譜分析化合物官能基
  • 平時考 Test
  • 作業 Assignment
  •  
    9 期中考 期中考 期中考  
    10 1H NMR Spectroscopy 1. Basic concepts
    2. The mechanism of resonance
    3. The chemical shift and shielding
    4. Local diamagnetic shielding
    5. Magnetic anisotropy
    6. Spin-spin splitting
    7. Survey of typical proton NMR absorption by type of compound
    學習如何以氫核磁共振光譜分析化合物結構
  • 作業 Assignment
  •  
    11 1H NMR Spectroscopy 1. Basic concepts
    2. The mechanism of resonance
    3. The chemical shift and shielding
    4. Local diamagnetic shielding
    5. Magnetic anisotropy
    6. Spin-spin splitting
    7. Survey of typical proton NMR absorption by type of compound
    學習如何以氫核磁共振光譜分析化合物結構
  • 作業 Assignment
  •  
    12 1H NMR Spectroscopy 1. Basic concepts
    2. The mechanism of resonance
    3. The chemical shift and shielding
    4. Local diamagnetic shielding
    5. Magnetic anisotropy
    6. Spin-spin splitting
    7. Survey of typical proton NMR absorption by type of compound
    學習如何以氫核磁共振光譜分析化合物結構
  • 作業 Assignment
  •  
    13 1H NMR Spectroscopy 1. Basic concepts
    2. The mechanism of resonance
    3. The chemical shift and shielding
    4. Local diamagnetic shielding
    5. Magnetic anisotropy
    6. Spin-spin splitting
    7. Survey of typical proton NMR absorption by type of compound
    學習如何以氫核磁共振光譜分析化合物結構
  • 作業 Assignment
  •  
    14 Carbon-13 NMR Spectra 1. Carbon-13 NMR shifts
    2. Proton-decoupled carbon-13 spectra
    3. Nuclear overhauser enhancement (NOE)
    4. A quick dip into DEPT
    5. Some sample spectra
    學習如何以碳-13核磁共振光譜分析化合物結構
  • 作業 Assignment
  •  
    15 Mass Spectrometry 1. The mass spectrum
    2. Determination of molecular weight
    3. Determination of molecular formula
    4. Some fragmentation patterns
    學習如何以質譜分析化合物結構  
    16 Compound analysis total analysis for experimental data 學習如何分析與判斷未知物的結構
  • 討論
  • 個別或小組指導
  • 講授
  • 平時考 Test
  • 作業 Assignment
  •  
    17 Compound analysis total analysis for experimental data 學習如何分析與判斷未知物的結構
  • 討論
  • 個別或小組指導
  • 講授
  • 平時考 Test
  • 作業 Assignment
  •  
    18 期末考 期末考 期末考
  • 期末考 Final Exam
  •  

    教學要點概述 Overview of Teaching Points:
    教材編選 Teaching Materials: □ 自編教材 Handout by Instructor □ 教科書作者提供 Textbook
    評量方法 Evaluation: 其他評量 Others:10%   問答 Interrogation:10%   報告 Presentation:30%   作業 Assignment:50%  
    教學資源 Teaching Resources: □ 教材電子檔 Soft Copy of the Handout or the Textbook □ 課程網站 Website
    教學相關配合事項 Other Matters Related to the Course:須修過普通化學、有機化學(一)(二)和儀器分析且皆通過的同學才能修課
    扣考規定 The rule of being able to take the final exam of the course:http://eboard.ttu.edu.tw/ttuwebpost/showcontent-news.php?id=504