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課程名稱 (中文) 定量分析
(英文) Quantitative Analysis
開課單位 化學工程學系
課程代碼 C4040
授課教師 黃燈輝
學分數 3.0 必/選修 選修 開課年級 大二
先修科目或先備能力:普通化學
課程概述與目標:概述:
說明分析化學的本質,定量分析中之誤差與隨意誤差在統計學上之處理,統計學上實驗數據之處理與評估:信賴區間與假設測試,樣品之取樣技巧、保存與標準化及檢量,電解質在平衡上之效應,多重平衡系統之求解方法,重量分析與應用,滴定方法與沉澱滴定及酸鹼的中和滴定,滴定曲線與酸鹼複合物之滴定與指示劑之使用及其變色範圍。
目標:
1. 使同學瞭解定量分析的原理並能活用於實際的分析化驗工作上。
2. 做儀器分析的前導課程,使同學充分瞭解分析工作的基本步驟。
教科書 Skoog/West/Holler/Crouch
Fundamentals of Analytical Chemistry
CENGAGE Learning, 2014, ISBN-13 : 978-1-305-04988-8
參考教材 Daniel C. Harris
Exploring Chemical Analysis, 5th Edition
Freeman and Company, ISBN-13 : 978-1-4292-9576-5
課程大綱 學生學習目標 單元學習活動 學習成效評量 備註
單元主題 內容綱要
1 The Analytical Process 1. The Analytical Chemist's Job
2. General Steps in Chemical Analysis
General Steps in Chemical Analysis
  • 講授
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    2 Chemical Measurements 1. SI Units and Prefixes
    2. Conversion Between Units
    3. Chemical Concentrations & Preparing Solution
    4. The Equilibrium Constant
    Chemical Measurements
  • 講授
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    3 Tools of the Trade 1. Safety with Chemicals and Waste
    2. Your Lab Notebook
    3. Glasswares and Aparatus
    4 Methods of Sample Preparation
    1. Safety with Chemicals and Waste
    2. Your Lab Notebook
    3. Glasswares and Aparatus
    4 Methods of Sample Preparation
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    4 Math Toolkit 1. Significant Figures & Types of Error
    2. Propagation of Uncertainty
    1. Significant Figures & Types of Error
    2. Propagation of Uncertainty
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    5 Statistics (I) 1. The Gaussian Distribution and Student's t
    2. Q Test for Bad Data
    1. The Gaussian Distribution and Student's t
    2. Q Test for Bad Data
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    6 Statistics (II) 1. Finding the Best Straight Line
    2. Constructing a Calibration Curve
    1. Finding the Best Straight Line
    2. Constructing a Calibration Curve
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    7 Good Titration (I) 1. Principles of Volumetric Analysis
    2. Titration Calculations
    Titration Calculations
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    8 Good Titration (II) Solubility Product and Titration of a Mixture Solubility Product and Titration of a Mixture
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    9 期中考週暫停一次 期中考週暫停一次 期中考週暫停一次
  • 期中考
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    10 Gravimetric and Combustion Analysis 1. Precipitation
    2. Gravimetric Calculations
    3. Combustion Analysis
    Gravimetric and Combustion Analysis
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  • 期中考訂正
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    11 Introducing Acids and Bases 1. What are Acids and Bases?
    2. pH definitions & [H+], [OH-] Relationship
    3. Dealing with Strong and Weak Acids and Bases
    4. Weak Acids and Bases Equilibrium
    Acids and Bases
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  • 作業
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    12 Buffers 1. The Henderson-Hasselbalch Equation
    2. Preparing Buffers and Buffer Capacity
    3. How Indicators Work
    Buffers and Buffer Capacity
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    13 Acid-Base Titration (I) Titration of Strong or Weak Acid with Strong Base Titration of Strong or Weak Acid with Strong Base
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    14 Acid-Base Titration (II) 1. Titration of Weak Base with Strong Acid
    2. Finding the End Point
    Titration of Weak Base with Strong Acid
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    15 Polyprotic Acids and Bases 1. Finding the pH in Diprotic Systems
    2. Which is the Principal Species?
    Polyprotic Acids and Bases
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  • 筆記
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    16 Polyprotic Acids and Bases Titrations in Polyprotic Systems Titrations in Polyprotic Systems
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  • 期末考
  • 到課率
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    17 A Deeper Look at Chemical Equilibrium 1. The Effect of Ionic Strength on Solubility of Salts
    2. Activity Coefficients
    3. Charge and Mass Balances
    Chemical Equilibrium
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  • 期末考訂正
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    18 期末考週暫停一次 期末考週暫停一次 期末考週暫停一次
  • 學期總成績
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